La2Mo2O9粉体的制备及表征
Synthesis and characterization of La2Mo2O9 powder
-
摘要: 本文采用溶胶-凝胶法和固相反应法制备La2Mo2O9粉体.采用XRD对不同方法制备的粉体的相组成进行了表征,结合TG-DTA结果确定了粉体烧结温度为600℃.SEM分析表明用柠檬酸盐法和固相反应法制备的粉体按1:1混合制成的样品的高温烧结性能得到改善.Abstract: EDTA and citric acid were used as chelating agent to synthesize La2Mo2O9 powder,respectively.XRD was used to study phase composition.Powder sintering temperature was determined by means of XRD and TG-DTA analysis.The sintering behaviors of the samples can be improved by mixing powders prepared by citrate method and solid state reaction method with a ratio of 1:1 as raw materials.