Abstract: In this paper, the importance of material analysis technology Course on the students majoring in materials was analyzed, and the design ideas of multimedia courseware are proposed according to the characteristics of material analysis technology course. The multimedia courseware of material analysis technology course is prepared using the software of Authorware, Flash MX, Photoshop, Premiere and so on. Meanwhile the corresponding technology of making multimedia courseware was discussed. The multimedia courseware has been used in teaching. Particularly, the animation operation demonstration form and video demonstration form of simulation experiment environment are adopted, and thus achieved a satisfactory teaching effect.