余小斌, 孟江燕, 范金娟, 魏振伟. SiCf/SiC复合材料原位分析研究进展[J]. 失效分析与预防, 2019, 14(5): 350-356. DOI: 10.3969/j.issn.1673-6214.2019.05.013
    引用本文: 余小斌, 孟江燕, 范金娟, 魏振伟. SiCf/SiC复合材料原位分析研究进展[J]. 失效分析与预防, 2019, 14(5): 350-356. DOI: 10.3969/j.issn.1673-6214.2019.05.013
    YU Xiao-bin, MENG Jiang-yan, FAN Jin-juan, WEI Zhen-wei. Research Progress of In-situ Analysis of SiCf/SiC Composites[J]. Failure Analysis and Prevention, 2019, 14(5): 350-356. DOI: 10.3969/j.issn.1673-6214.2019.05.013
    Citation: YU Xiao-bin, MENG Jiang-yan, FAN Jin-juan, WEI Zhen-wei. Research Progress of In-situ Analysis of SiCf/SiC Composites[J]. Failure Analysis and Prevention, 2019, 14(5): 350-356. DOI: 10.3969/j.issn.1673-6214.2019.05.013

    SiCf/SiC复合材料原位分析研究进展

    Research Progress of In-situ Analysis of SiCf/SiC Composites

    • 摘要: 原位观测方法能实时、动态、连续地观测SiCf/SiC复合材料的损伤演变过程,对研究SiCf/SiC复合材料在服役环境下的安全运行具有重要的学术价值和工程意义。本文介绍了SEM原位观测、X-CT原位观测、TEM原位观测方法的原理及在研究SiCf/SiC复合材料损伤演变方面的优势、局限性及制样方法,综述了近年来国内外采用SEM、X-CT及TEM 3种原位观测方法分析SiCf/SiC复合材料微裂纹的萌生、扩展过程及微观结构对于不同外部激励信号的动态响应过程的研究工作。最后指出X-CT原位分析技术研究SiCf/SiC复合材料的动态损伤是未来的主要发展方向。

       

      Abstract: The in-situ observation method can observe the damage evolution process of continuous silicon carbide fibers reinforced silicon carbide ceramic composites (SiCf/SiC) in real time, dynamically and continuously, so it is of important academic value and high engineering significance to the study of the safe operation of SiCf/SiC composites in application. The principles of scanning electron microscopy(SEM), X-ray computed tomography(X-CT), and transmission electron microscopy(TEM) in-situ observation and their advantages, limitations and specimen preparation methods in the study of mechanical damage evolution of SiCf/SiC composites were introduced firstly. SEM, X-CT and TEM in-situ observation methods have been widely used to analyze microcrack initiation and propagation in SiCf/SiC composites, as well as the dynamic response process of microstructure to different external excitation signals in recent years. These researches were reviewed. Finally, it was pointed out that X-CT in-situ analysis technology would have a wonderful future in the study of dynamic damage of SiCf/SiC composite in the future.

       

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