韩梅, 岳晓岱, 董建民, 谢洪吉, 李嘉荣. DD6单晶高温合金初熔组织演变机制研究[J]. 失效分析与预防, 2019, 14(3): 166-171. DOI: 10.3969/j.issn.1673-6214.2019.03.006
    引用本文: 韩梅, 岳晓岱, 董建民, 谢洪吉, 李嘉荣. DD6单晶高温合金初熔组织演变机制研究[J]. 失效分析与预防, 2019, 14(3): 166-171. DOI: 10.3969/j.issn.1673-6214.2019.03.006
    HAN Mei, YUE Xiao-dai, DONG Jian-min, XIE Hong-ji, LI Jia-rong. Evolutionary Mechanism of Incipient Melting Microstructure of Single Crystal Superalloy DD6[J]. Failure Analysis and Prevention, 2019, 14(3): 166-171. DOI: 10.3969/j.issn.1673-6214.2019.03.006
    Citation: HAN Mei, YUE Xiao-dai, DONG Jian-min, XIE Hong-ji, LI Jia-rong. Evolutionary Mechanism of Incipient Melting Microstructure of Single Crystal Superalloy DD6[J]. Failure Analysis and Prevention, 2019, 14(3): 166-171. DOI: 10.3969/j.issn.1673-6214.2019.03.006

    DD6单晶高温合金初熔组织演变机制研究

    Evolutionary Mechanism of Incipient Melting Microstructure of Single Crystal Superalloy DD6

    • 摘要: 分析第二代单晶高温合金DD6在略高于固溶热处理窗口的温度1 330 ℃下保温的初熔组织演变。结果表明:保温0.5 h后,枝晶间发生明显初熔,并大量形成典型初熔组织,部分初熔组织中心形成显微孔洞;随保温时间延长,初熔逐渐消退并演变为正常合金组织;保温8 h后,初熔组织完全消失,仅留下初熔形成的微孔。应用热力学、动力学计算分析试验结果可知:DD6合金在铸态下枝晶偏析显著,枝晶间固相线温度明显低于枝晶干,在略高于枝晶间固相线的温度下保温,初始阶段枝晶间发生初熔;继续保温,元素均匀化程度改善,枝晶间固相线温度升高,初熔组织逐渐消退,最终演变为正常合金组织。

       

      Abstract: The evolution of the incipient melting microstructure of the second-generation single crystal superalloy DD6 was studied during heat treatment at 1 330 ℃, slightly higher than its solution heat treatment window. After heat treated for 0.5 h, incipient melting occurs at interdendrites, and some of the incipient melting regions have a pore at the center; with the holding time increasing, incipient melting microstructure fades away gradually and totally disappears after 8 h. The experimental results are analyzed by thermodynamic and kinetic calculations. The solidus temperature of the interdendrite region of as-casting DD6 single crystal superalloy is apparently lower than that of the dendrite arm region because of severe dendrite segregation. During the heat treatment at a temperature slightly higher than the solidus temperature, incipient melting occurs initially; it fades away gradually with the improvement of element homogenization degree, and finally turns to normal microstructure.

       

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